Multicatalytic Enantioselective Borrowing Hydrogen delta-Lactonization Strategy from beta-Keto Esters and Allylic Alcohols

By combining an iron-catalyzed borrowing hydrogen of allylic alcohols with an enantioselective organocatalyzed Michael addition of β-keto esters followed by a subsequent DBU-promoted lactonization different enantioenriched δ-lactones have been synthesized with good enantioselectivities. The valuable building blocks, featuring in some cases challenging quaternary stereocenters, have been obtained with >90% ee.

Références

Titre
Multicatalytic Enantioselective Borrowing Hydrogen delta-Lactonization Strategy from beta-Keto Esters and Allylic Alcohols
Type de publication
Article de revue
Année de publication
2018
Revue
Synthesis
Volume
50
Ticket
4
Pagination
785–792
ISSN
0039-7881 DOI - 10.1055/s-0036-1588547
Soumis le 7 septembre 2022